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| 康偶酰的合成研究 |
| Study on Synthesis of α, α'-Furil |
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| DOI：10.3969/j.issn.1671-5322.2007.04.015 |
| 中文关键词: 康偶酰 氧化 醋酸铜 |
| 英文关键词: α,α’-Furil oxidation cupric acetate |
| 基金项目: |
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| 摘要点击次数: 4655 |
| 全文下载次数: 3979 |
| 中文摘要: |
| 研究了用醋酸铜氧化法制备康偶酰,讨论了康料配比、水的用量、温度、时间等因素对反应的影响,对康偶酰制备的工艺参数进行优化,收率达到97.2%,均超过了传统方法,且简化了工艺,缩短了反应时间,易于工业化生产. |
| 英文摘要: |
| The process of using cupric acetate to pre-α,α’-Furil is studied.Tempreture,time,quantity of water and cupric acetate are also obseverd for getting the optimal zeaction condition.A parameter design method is applied to select the optimum synthesis conditions.97.2% yields superior to the conventional for pre-α,α’-Furil are obtained respectively.Besides,the process is simplified,the time shortened,and production industrialized easily. |
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